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Magnetism Reflectometer Frequently Asked Questions

1.) How do I arrange to do an experiment at SNS?

 

1) Here are some instructions for arranging beam time at SNS:

  • Submit a proposal. Go to the User Info page and use the link under Resources to get to the ORNL Neutron Science User Program web site. Read the information, especially the Policies and Guidelines.  Follow the instructions on how to become an SNS user, as well as important information concerning site access, training, experiment and sample handling.  The User Info page also has a link with Instructions for Accessing the Integrated Proposal Tracking System.  Use this link, and follow the instructions to submit a proposal.
  • Register. Once your proposal has been accepted, contact the Users Office as soon as possible.  Please note that for citizens of certain countries it can take up to eight weeks to arrange site access.  This may affect the scheduling of your beam time, so contact the user office as soon as possible.
  • Arrange dates. You will be contacted by the Magnetism Reflectometer Instrument Scientist to arrange specific dates for your beam time.
  • Arrange Travel and accommodations.  Make your travel arrangements and reserve your hotel accommodations.  Information on Oak Ridge hotels is available on the Visitor Info page.
  • Confirm. Finally, contact the Users Office to confirm dates and arrangements for your visit.

2) What size samples can I bring?

 

2) Maximum sample size is limited by sample environment requirements:

  • Samples run at room temperature with no magnetic field have virtually no restrictions.
  • Samples run at room temperature that are placed within the electromagnet pole pieces have a maximum height of 100 millimeters.
  • Samples run at low temperature require mounting inside our closed cycle helium refrigerator, and have a maximum size of 20 x 20 millimeters.

Minimum sample size is approximately 10 X 10 millimeters.  Sample sizes smaller that this will generally require more beam time than is reasonable for a fully subscribed instrument.


3) What sample thickness can I study?

 

3) Film thickness oscillations can usually be resolved for thicknesses ranging from a few monolayers up to approximately 7000 Å.

4) What do I do if I want my samples returned to me?

 

4) If you are present at the SNS when your samples are run and they have been cleared by the Radiological Control Group, you can carry them back with you.  If you are not present, or you leave before one of your samples is completed, we can ship samples back to you once they have been cleared by the Radiological Controls Group, provided we have a complete shipping address, with phone number, a complete MSDS for the sample and a Fed Ex (or other shipping service) account number to which the shipment will be billed. 

5) What range of temperatures and magnetic fields can I run at?

 

5) The beam line 4A closed cycle helium refrigerator has a temperature range between 4.2 and 450 Kelvin.  To accommodate the refrigerator (which accommodates 20 X 20 millimeter samples), the magnet pole pieces are placed 50 millimeters apart, which limits the maximum magnetic field to approximately 1.2 Tesla.  For samples approaching the minimum sample size (10 X 10 millimeters) running at room temperature and mounted outside the refrigerator the pole piece gap can be reduced, which increases the maximum field to approximately 3 Tesla.

6) Hey, where did the beam go?

 

6) While the SNS facility operates seven days a week, twenty four hours a day during normal operations, there are scheduled periods during operations cycles when the SNS does not produce neutrons for users (maintenance periods and accelerator physics schedules).  No data will be collected during these periods. This is normal.  Check the long term run schedule to view the listing of these periods.

Beam Line 4a Team Site (password required)

 

 
  Information Contact : Rick Goyette - goyetterj@sns.gov  

Oak Ridge National Laboratory

Office of Science